| |
| Previous course: C2337 |
| Offered by:
Department of Organic Chemistry
(OK) |
| No credit points with: C2337 |
| Compulsory: 23117/C2317/C2319 |
| Prerequisite: 23220/C2320 |
| Desirable: 23352/C2352 |
| Recommended semester:
6th-10th semester |
| Limitation: Max. 12 |
| Scope and form: Lectures, laboratory work and seminars. |
| Examination:
Approval of oral presentation of results, journals, homework assignments and reports
(
pass/fail
) |
| Contact person: |
Jørgen Øgaard Madsen, OK, Building 201, Tel. +45 4525 2155
Bo Werner Christensen, OK, Building 201, Tel. +45 4525 2105 |
|
| Aim: To enable the participants to choose and to optimise chromatographic methods for the analysis of complicated mixtures of organic compounds in conjunction with mass spectrometry and possibly NMR-spectroscopy. |
| Contents: An introduction to the theory of gas and liquid chromatography. Manufacturing and testing of columns for analytical and preparative purposes,separation, structure determination and quantification of small amounts of organic substances in complicated mixtures: gas chromatography/ mass spectrometry in connection with a computer and liquid chromatography in connection with Fourier transform 1H NMR.The samples may be derived from current problems in research projects at the Department, isolation of natural products, industrial processes, and environmental investigations. Methods for extraction and pretreatment of samples (e.g. small amounts of organic matter in air or aqueous solution) are assessed and practiced. |
