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21525 Basic Methods in X-ray Diffractometry and Optical Crystallography
Danish title: Elementære røntgenkrystallografiske og krystaloptiske analysemetoder
Language: Danish Credit points: 5
Type: Open University
Language: Danish

Previous course: C3506
No credit points with: C3501/C3503/C3506
Recommended semester: 1st - 4th semester
Scope and form: 3 week period with laboratory work 7 hours a day and home work 1 hour a day.
Examination: Evaluation of report(s) (Pass/fail)
Participant limitation: max. 16

Remarks: The course is a valuable basis for studying crystalline materials.
Contact person: Inger Lise Gerhard Olsen, Building 206, Tel. +45 4525 2264, email ilo@kemi.dtu.dk
Sven Karup-Møller, Building 204, Tel. +45 4525 2228, email iggskm@pop.dtu.dk

Department: Department of Chemistry
Aim: To enable the participants to identify pure substances and mixtures of few components using X-ray powder methods, and to familiarize the participants with the use of the polarizing microscope for identifying crystalline substances in transmitted light. The course has been organised with the aim of using these methods for control of raw materials and the solution of other material problems in industry.
Contents: The course is split into two parts of equal length. One part covers powder diffractometry using a Philips diffractometer and the Debye-Scherrer and Gandolfi methods. Identification of pure substances and mixtures using a reference work, identification indices for X-ray reflections and calculation of cell constants of simple substances. The other part of the course deals with the use of the polarisation microscope. Determination of optical properties of solids in transmitted light, such as pleochroism, refraction and double refraction for fast identification of crystalline substances.